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METHOD OF PREPARING GRAPHENE-COATED ALUMINA AND GRAPHENE-COATED ALUMINA PREPARED USING THE METHOD

机译:制备石墨烯包覆的氧化铝的方法以及使用该方法制备的石墨烯包覆的氧化铝

摘要

A method of preparing graphene-coated alumina, the method including: (1) preparing a liquid polyacrylonitrile (LPAN) solution, stirring the LPAN solution at between 100 and 200° C. to yield a cyclized polyacrylonitrile solution; (2) heating the cyclized LPAN solution at between 200 and 300° C. to yield a thermally-oxidized polyacrylonitrile (OPAN) having a ladder structure; (3) mixing the thermally-oxidized polyacrylonitrile with an aluminum compound, to yield a mixture, and adding a solvent to the mixture, uniformly mixing, to yield a polyacrylonitrile-coated aluminum compound; (4) drying the polyacrylonitrile-coated aluminum compound until the solvent is evaporated, to yield a carbonized precursor-coated aluminum compound; and (5) calcining the carbonized precursor-coated aluminum compound in the presence of an inert gas flow, to yield graphene-coated alumina.
机译:一种制备石墨烯包覆的氧化铝的方法,该方法包括:(1)制备液态聚丙烯腈(LPAN)溶液,在100至200℃之间搅拌该LPAN溶液以产生环化聚丙烯腈溶液。 (2)在200〜300℃之间加热环化的LPAN溶液,得到具有梯形结构的热氧化聚丙烯腈(OPAN)。 (3)将热氧化聚丙烯腈与铝化合物混合,得到混合物,并向该混合物中加入溶剂,均匀混合,得到聚丙烯腈包覆铝化合物。 (4)干燥涂覆有聚丙烯腈的铝化合物,直到蒸发掉溶剂,得到碳化的涂覆有前体的铝化合物。 (5)在惰性气流的存在下煅烧碳化的涂覆有前体的铝化合物,得到石墨烯涂覆的氧化铝。

著录项

  • 公开/公告号US2016189819A1

    专利类型

  • 公开/公告日2016-06-30

    原文格式PDF

  • 申请/专利权人 JIANHONG LIU;

    申请/专利号US201514981989

  • 申请日2015-12-29

  • 分类号H01B1/02;H01B13;C09K5/14;

  • 国家 US

  • 入库时间 2022-08-21 14:34:06

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