首页> 外国专利> METHOD FOR PREPARING MACRO/MICRO DUAL POROUS STRUCTURE-TYPE THREE-DIMENSIONAL POROUS SUPPORT, AND MACRO/MICRO DUAL POROUS STRUCTURE-TYPE THREE-DIMENSIONAL POROUS SUPPORT PREPARED THEREBY

METHOD FOR PREPARING MACRO/MICRO DUAL POROUS STRUCTURE-TYPE THREE-DIMENSIONAL POROUS SUPPORT, AND MACRO/MICRO DUAL POROUS STRUCTURE-TYPE THREE-DIMENSIONAL POROUS SUPPORT PREPARED THEREBY

机译:制备宏/微对偶多孔结构型三维多孔体的方法及由此制备的宏/微对偶多孔结构型三维多孔体

摘要

The present invention relates to a method for preparing a macro/micro dual porous structure-type three-dimensional porous support, comprising the steps of: pouring, into a cylindrical mold, a precursor material constituting a porous body, a dispersant and a freezing medium, freeze casting the same at or below the freezing point of the freezing medium, and then extruding the same; layering a fiber, to be extruded in the prior step, into a desired shape through a 3D robot; and pressurizing the layered product at a specific temperature, and then removing the freezing medium by freeze-drying the same. A three-dimensional porous support prepared by the preparation method according to the present invention has excellent inner connecting pores and has a dual porous structure of a micropore and a macropore, and the pore size can be controlled by using a remelting phenomenon of a freezing medium. In addition, a complex structure can be directly prepared by using a 3D robot instead of a conventional method of indirectly preparing a complex structure by using a mold.
机译:本发明涉及一种制备宏观/微观双重多孔结构型三维多孔载体的方法,其包括以下步骤:将构成多孔体的前体材料,分散剂和冷冻介质倒入圆柱形模具中。 ,在冷冻介质的冰点或低于冰点的温度下将其冷冻浇铸,然后将其挤出;通过3D机械手将要在先前步骤中挤出的纤维分层成所需的形状;将层状产品在特定温度下加压,然后通过冷冻干燥除去冷冻介质。通过本发明的制备方法制备的三维多孔载体具有优异的内部连接孔,并且具有微孔和大孔的双重多孔结构,并且可以通过使用冷冻介质的重熔现象来控制孔径。 。另外,可以通过使用3D机器人直接制备复杂结构,而不是通过使用模具间接制备复杂结构的常规方法。

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