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AQUEOUS SYNTHESIS OF NANOPARTICLES OF CADMIUM SULPHIDE

机译:硫化镉纳米粒子的水合成

摘要

The invention relates to a method for the synthesis of fluorescent, semiconductive nanoparticles (NPs) of cadmium sulphide (CdS), comprising: a) mixing i. a thiol as a source of sulphur and as a covering compound; ii. a cadmium sa iii. a compound containing or generating a source of phosphate; b) adding a buffer solution to the mixture obtained in step (a), at a pH of between 7 and 10, in the presence or absence of oxygen and at a temperature of between 15 and 80°C; c) incubating the solution produced in b) at a temperature of between 15 and 80°C, for an incubation period of between 1 and 9 days, until fluorescence is obtained; and d) evaluating the fluorescence of the NPs of CdS, exposing them to a UV transilluminator (at 365 nm).
机译:本发明涉及一种用于合成硫化镉(CdS)的荧光的半导体纳米颗粒(NP)的方法,该方法包括:a)混合i。硫醇作为硫的来源和覆盖化合物; ii。镉盐; iii。含有或产生磷酸盐源的化合物; b)在有氧或无氧条件下,在15至80℃之间,在7至10之间的pH下,向步骤(a)中获得的混合物中加入缓冲溶液; c)将b)中产生的溶液在15至80℃的温度下温育1至9天,直到获得荧光; d)评估CdS NP的荧光,将其暴露于UV透照器(在365 nm)。

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