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METHOD FOR PREPARING LIGNIN-MODIFIED FURAN RESIN

机译:木质素改性的呋喃树脂的制备方法

摘要

Disclosed are a method for preparing lignin-modified furan resin and the lignin-modified furan resin prepared by using the method. The method of the present invention comprises: step 1, adding formaldehyde into a reaction vessel, adjusting the PH to be alkaline, adding lignin, and reacting under the action of stirring; step 2, adding carbamide for reaction; step 3, adding furfuryl alcohol, reacting under an alkaline condition, and adjusting the PH to be acid for reaction; and step 4, adding carbamide for reaction, dewatering a system under the condition of vacuum, adding furfuryl alcohol into the dewatered system, and stirring the system to be uniform to obtain the lignin-modified furan resin. The furan resin prepared by using the method of the present invention is low in content of free furfuryl alcohol and free formaldehyde, and the emission of formaldehyde in the casting and mulling process can be effectively reduced, so that requirements on environmentally-friendly furan resin are met.
机译:本发明公开了一种木质素改性的呋喃树脂的制备方法和使用该方法制备的木质素改性的呋喃树脂。本发明的方法包括:步骤1,将甲醛加入反应容器中,调节PH为碱性,加入木质素,在搅拌作用下反应;步骤2,加入尿素进行反应。步骤3,加入糠醇,在碱性条件下反应,调节PH为酸进行反应。步骤4,加入氨基甲酸酯进行反应,在真空条件下使体系脱水,向脱水体系中加入糠醇,搅拌均匀,得到木质素改性的呋喃树脂。通过本发明的方法制备的呋喃树脂的游离糠醇和游离甲醛含量低,可以有效减少流延和成糊过程中甲醛的排放,从而降低了对环保型呋喃树脂的要求。遇见。

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