首页> 外国专利> RDX RDX PREPARATION METHOD FOR SUBMICRON AND MICRON SIZE- SPHERICAL RDX PARTICLES AND SPHERICAL RDX PARTICLES PREPARED BY THE SAME

RDX RDX PREPARATION METHOD FOR SUBMICRON AND MICRON SIZE- SPHERICAL RDX PARTICLES AND SPHERICAL RDX PARTICLES PREPARED BY THE SAME

机译:亚微米和亚微米尺寸的RDX RDX的制备方法-球形RDX颗粒和相同制备的球形RDX颗粒

摘要

The present invention relates to a method for manufacturing a submicron and micron-sized spherical RDX (cyclotrimethylene trinitramine) particle and a spherical RDX particle manufactured thereby. More specifically, the method for manufacturing the submicron and micron-sized spherical RDX particle comprises: a step for manufacturing an RDX solution by dissolving RDX in an organic solvent; a step for precipitating an RDX particle by mixing the RDX solution with an antisolvent; and a step for obtaining the precipitated RDX particle. Before the RDX solution and the antisolvent are mixed, a surfactant is added to the RDX solution or the antisolvent to be mixed. According to the present invention, a submicron and micron-sized spherical RDX particle is manufactured with productivity higher than that of a conventional method. In the case of a spherical shaped RDX particle, ignition pressure can be maximized due to increase in filling density and a relatively insensitive RDX particle can be manufactured due to a smooth surface. In addition, due to a size of a fine particle, an energy release rate is high, whereby it can be widely used as a civil and military composition such as high explosive gunpowder, a solid composite propellant, and the like.
机译:本发明涉及用于制造亚微米和微米尺寸的球形RDX(环三亚甲基三硝胺)颗粒的方法以及由此制备的球形RDX颗粒。更具体地,用于制造亚微米和微米尺寸的球形RDX颗粒的方法包括:通过将RDX溶解在有机溶剂中来制造RDX溶液的步骤;通过将RDX溶液与抗溶剂混合来沉淀RDX颗粒的步骤;获得沉淀的RDX颗粒的步骤。在将RDX溶液和抗溶剂混合之前,将表面活性剂加入到RDX溶液或抗溶剂中进行混合。根据本发明,以比常规方法更高的生产率制造亚微米和微米尺寸的球形RDX颗粒。在球形RDX颗粒的情况下,由于填充密度的增加可以使点火压力最大化,并且由于光滑的表面可以制造相对不敏感的RDX颗粒。另外,由于微粒的尺寸,能量释放率高,从而其可以广泛地用作民用和军用组合物,例如高炸药火药,固体复合推进剂等。

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