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METHOD FOR SEPARATION OF GOLD-SILVER ALLOYS BY VACUUM DISTILLATION AND DEVICE FOR ITS IMPLEMENTATION

机译:真空蒸馏分离金银合金的方法及其实施装置

摘要

1. A method for separating gold-silver alloys by vacuum distillation, including heating the feedstock under high vacuum to the temperature of evaporation of the volatile components from its melt surface and their solid state transition in the condensation zone of the cooled condenser, characterized in that the condensation of metals from the vapor-gas mixture occurs in a limited the area of the cooled condenser with strictly directed movement of the vapor-gas mixture flow from the crucible to the condensation zone, which increases the pressure of the vapor-gas mixture, subject to the relation: T T, where T is the condensation temperature, T is the melting temperature of the deposited metal, creating the conditions for the appearance of a significant number of nucleation centers of crystallization. 2. Installation for implementing a method for separating gold-silver alloys by vacuum distillation, including a vacuum chamber 1 in which a melting crucible 2 is placed, around the crucible there is a heating element 4 in the form of an inductor made with a rotary device and the possibility of tipping at least one capacitor 5 with several traps 6 and mold 7, characterized in that it is additionally equipped with a heat shield 8 located between the winding of the inductor and the crucible, on top of which a conical nozzle is installed 3.3. Vacuum distillation unit for separating gold-silver alloys according to claim 2, characterized in that the capacitor is made in the form of a hemisphere. 4. A vacuum distillation unit for separating gold-silver alloys according to claim 2, characterized in that the conical nozzle is made of graphite. 5. Vacuum Distillation Unit for Separating Gold-Silver Alloys
机译:1.一种通过真空蒸馏分离金银合金的方法,包括在高真空下将原料加热至挥发性组分从其熔融表面的蒸发温度,以及在冷却的冷凝器冷凝区中的固态转变,其特征在于:蒸气混合物中金属的冷凝发生在冷却冷凝器的有限区域内,蒸气混合物流从坩埚到冷凝区的方向严格,这会增加蒸气混合物的压力,取决于下列关系式:T <T,其中T是缩合温度,T是沉积金属的熔化温度,这为出现大量结晶成核中心创造了条件。 2.一种用于实施通过真空蒸馏分离金银合金的方法的设备,包括在其中放置有熔融坩埚2的真空室1,在坩埚周围,存在由感应器形式的加热元件4,该感应器由旋转式制成。该装置以及使至少一个电容器5具有多个阱6和模具7倾倒的可能性,其特征在于,该电容器另外还配备有位于感应器的绕组和坩埚之间的隔热罩8,在该隔热罩的顶部是锥形喷嘴。已安装3.3。 3.根据权利要求2所述的用于分离金银合金的真空蒸馏单元,其特征在于,所述电容器以半球的形式制成。 4.根据权利要求2所述的用于分离金银合金的真空蒸馏单元,其特征在于,所述锥形喷嘴由石墨制成。 5.分离金银合金的真空蒸馏装置

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