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The method for determining the content of extractable organic compounds in sediment samples

机译:沉积物样品中可萃取有机物含量的测定方法

摘要

A method for determining the content of extractable organic compounds in sediment samples, comprising the steps that a sample of sediment were placed in a flask produce extraction methylene chloride, and the content of extractable organic compounds is determined after filtering the resulting extract, characterized in that methylene chloride is introduced into the flask with the portion of bottom Fat from a 5 ml methylene chloride per 1 g of the sample, extraction is carried out with placing the flask in an ultrasonic bath for 15 minutes, the extract is filtered in Khim sky glass using a filter, transmissive dispersion medium and retarding the dispersed solid phase, and then extraction is carried out stripping of methylene chloride by pouring the filtered extract by parts in a preweighed weighing bottle until they reach a constant weight, wherein the content of extractable organic compounds in the sample is determined by the difference weights pure and the filled weighing bottle.
机译:一种测定沉积物样品中可萃取有机物含量的方法,包括将沉淀物样品置于烧瓶中产生二氯甲烷的步骤,并在过滤所得萃取物后确定可萃取有机化合物的含量,其特征在于:将二氯甲烷与每1克样品中5毫升二氯甲烷中的一部分底部脂肪一起引入烧瓶中,将烧瓶置于超声浴中15分钟进行提取,提取物在Khim Sky玻璃中过滤使用过滤器,透射型分散介质并延迟分散的固相,然后通过将过滤后的提取物分批倒入预先称重的瓶中直至达到恒重来进行萃取,以进行二氯甲烷的汽提。其中,可萃取有机化合物的含量样品中的重量由纯净重量和填充的称量瓶确定。

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