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MANUFACTURING METHOD OF MSE TYPE ZEOLITE

机译:MSE型沸石的制造方法

摘要

PROBLEM TO BE SOLVED: To provide a manufacturing method of MSE type zeolite capable of manufacturing the MSE type zeolite with a relatively short heating time by using inexpensive tetraethylammonium ion.SOLUTION: There is provided a manufacturing method of MSE type zeolite including (1) mixing a silica source, an alumina source, an alkali source, tetraethylammonium ion and water to prepare a reaction mixture with a composition represented by a molar ratio described as SiO/AlO=10-100, (NaO+KO)/SiO=0.15-0.50, KO/(NaO+KO)=0.05-0.7, TEAO/SiO=0.08-0.20, HO/SiO=5-50, (2) adding MSE type zeolite seed crystal to the mixture at a ratio of 5-30 mass% based on the silica component and (3) heating the reaction mixture to which the seed crystal is added at a temperature of 100-200°C under a sealed condition.SELECTED DRAWING: Figure 8
机译:解决的问题:提供一种能够通过使用廉价的四乙基铵离子在较短的加热时间下制造MSE型沸石的MSE型沸石的制造方法。解决方案:提供一种包括(1)混合的MSE型沸石的制造方法。二氧化硅源,氧化铝源,碱源,四乙基铵离子和水制备反应混合物,其组成的摩尔比表示为SiO / AlO = 10-100,(NaO + KO)/SiO=0.15-0.50 ,KO /(NaO + KO)= 0.05-0.7,TEAO / SiO = 0.08-0.20,HO / SiO = 5-50,(2)以5-30质量%的比例向混合物中添加MSE型沸石晶种(3)在密闭条件下于100-200°C的温度下加热加入了晶种的反应混合物(图3)。

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