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Method for preparing NaY molecular sieve of high silica-alumina ratio and product thereof

机译:高硅铝比NaY分子筛的制备方法及其产品

摘要

A method for preparing a NaY molecular sieve having a high silica-to-alumina ratio, wherein deionized water, a silicon source, an aluminum source, an alkali source, and ILs as a template agent are mixed to obtain an initial gel mixture; the initial gel mixture is maintained at a proper temperature and aged, then fed into a high pressure synthesis kettle for crystallization; the solid product is separated and dried, to obtain the NaY molecular sieve having a high silica-to-alumina ratio, wherein the ILs is a short-chain alkylimidazolium ionic liquid, the template agent is less volatile, and the resultant high-silicon Y molecular sieve has a high crystallinity and a silica-to-alumina ratio of 6 or more.
机译:一种高硅铝比NaY分子筛的制备方法,其中将去离子水,硅源,铝源,碱源和ILs作为模板剂混合,得到初始凝胶混合物。将最初的凝胶混合物保持在适当的温度并老化,然后加入高压合成釜中结晶。分离并干燥固体产物,以获得具有高的硅铝比的NaY分子筛,其中IL是短链烷基咪唑鎓离子液体,模板剂的挥发性较小,并且所得的高硅Y分子筛具有高结晶度,二氧化硅与氧化铝之比为6或更高。

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