首页> 外国专利> METHOD FOR PRODUCTION OF HEAT-RESISTANT, SUPERHARD COMPOSITE MATERIAL ON THE BASIS OF MODIFIED DIAMOND AND CUBIC BORON NITRIDE POWDERS

METHOD FOR PRODUCTION OF HEAT-RESISTANT, SUPERHARD COMPOSITE MATERIAL ON THE BASIS OF MODIFIED DIAMOND AND CUBIC BORON NITRIDE POWDERS

机译:以改性金刚石和立方氮化硼粉为基础的耐热,高温复合材料的生产方法

摘要

The invention is related to the field of production of superhard composite diamond materials and is intended for manufacture of dressing, shape-forming and edge cutting tools. The method comprises annealing of powders of diamond and cubic boron nitride in a protective atmosphere, in vapour of silicon-containing compounds followed by sintering of the blend produced under conditions of high pressures and temperatures; in accordance with the invention, diamond powder is annealed at a temperature of 850-1000°C during 1-4 hours; after annealing, silicon quantity on diamond powder grains is within 8-30% by mass of initial mass of diamond powder; cubic boron nitride powder is annealed at a temperature of 850-1000°C during 1-2 hours, after annealing, silicon quantity on cubic boron nitride powder grains is within 8-15% by mass of initial mass of cubic boron nitride powder; grain size in diamond and cubic boron nitride powders is within 1-40 μm, the ratio of diamond powder mass to cubic boron nitride powder mass in the blend is within 1:1 to 5:1, and blend sintering at high pressures and temperatures is performed at a pressure range of 5.0-6.0 GPa at a temperature of 1650-2000°C during 30-60 s. To improve sintering behaviour of the material, amorphous boron powder in an amount of 0.5-1.5% by mass and/or aluminium powder in an amount of 1-5% by mass is added to the blend of diamond and cubic boron nitride powders. The use of the present invention makes it possible to decrease the cost of the superhard material production process and to improve physico-mechanical and cutting properties of tools based thereon.
机译:本发明涉及超硬复合金刚石材料的生产领域,并且用于制造修整,成形和切边工具。该方法包括在保护性气氛中在含硅化合物的蒸气中将金刚石和立方氮化硼的粉末退火,然后烧结在高压和高温条件下产生的混合物。根据本发明,将金刚石粉末在850-1000℃的温度下退火1-4小时。退火后,金刚石粉晶粒上的硅含量为金刚石粉初始质量的8-30质量%。将立方氮化硼粉末在850-1000℃的温度下退火1-2小时,退火后,立方氮化硼粉末晶粒上的硅含量为立方氮化硼粉末初始质量的8-15质量%。金刚石和立方氮化硼粉末的晶粒尺寸在1-40μm之内,共混物中金刚石粉末质量与立方氮化硼粉末质量之比在1:1至5:1之内,在高压和高温下的共混物烧结为在16-50-2000°C的温度下于5.0-6.0 GPa的压力范围内执行30-60 s。为了改善材料的烧结性能,将0.5质量%至1.5质量%的无定形硼粉末和/或1-5质量%的铝粉末添加至金刚石和立方氮化硼粉末的共混物中。本发明的使用使得可以降低超硬材料生产过程的成本,并且可以改善基于其的工具的物理机械和切削性能。

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