首页> 外国专利> METHOD FOR PRODUCING N-SUBSTITUTED CARBAMIC ACID ESTER, METHOD FOR PRODUCING ISOCYANATE USING N-SUBSTITUTED CARBAMIC ACID ESTER, AND COMPOSITION FOR TRANSFERRING AND STORING N-SUBSTITUTED CARBAMIC ACID ESTER CONTAINING N-SUBSTITUTED CARBAMIC ACID ESTER AND AROMATIC HYDROXY COMPOUND

METHOD FOR PRODUCING N-SUBSTITUTED CARBAMIC ACID ESTER, METHOD FOR PRODUCING ISOCYANATE USING N-SUBSTITUTED CARBAMIC ACID ESTER, AND COMPOSITION FOR TRANSFERRING AND STORING N-SUBSTITUTED CARBAMIC ACID ESTER CONTAINING N-SUBSTITUTED CARBAMIC ACID ESTER AND AROMATIC HYDROXY COMPOUND

机译:制备N-取代的碳酸酯的方法,使用N-取代的碳酸酯生产异氰酸酯的方法,以及转移和储存包含N-取代的碳酸酯和芳族混合羟基的N-取代的碳酸酯的组合物

摘要

Provided is a method for producing an N-substituted carbamic acid ester derived from an organic amine from an organic amine, a carbonic acid derivative, and a hydroxy compound containing one or more hydroxy compounds. The method comprises: reacting the organic amine, the carbonic acid derivative, and the hydroxy composition using a reactor for producing urethane provided with a condenser; and condensing the hydroxy composition and a compound having a carbonyl group derived from the carbonic acid derivative by introducing the hydroxy composition, the compound having a carbonyl group derived from the carbonic acid derivative, and air containing ammonia produced as a by-product in the reaction into the condenser attached to the reactor for producing urethane. The stoichiometric ratio of the hydroxy compound contained in the hydroxy composition to be condensed to the compound having a carbonyl group derived from the carbonic acid derivative to be condensed is 1 or more, and the ratio of the number of carbonyl groups (-C(=O)-) contained in the compound having a carbonyl group derived from the carbonic acid derivative incorporated in ammonia to be collected as gas by the condenser to the number of ammonia molecules is 1 or less.
机译:提供一种从有机胺,碳酸衍生物和含有一种或多种羟基化合物的羟基化合物制备由有机胺衍生的N-取代氨基甲酸酯的方法。该方法包括:使用具有冷凝器的用于生产氨基甲酸酯的反应器使有机胺,碳酸衍生物和羟基组合物反应。通过引入羟基组合物,将羟基组合物与具有衍生自碳酸衍生物的羰基的化合物进行缩合,使具有碳酸衍生物的羰基的化合物和含有氨的空气作为副产物在反应中冷凝。进入连接到用于生产氨基甲酸酯的反应器的冷凝器中。缩合的羟基组合物中所含的羟基化合物与衍生自缩合的碳酸衍生物的具有羰基的化合物的化学计量比为1以上,且羰基数的比(-C(=包含在羰基中的具有羰基的化合物中的O)-)包含在氨中,该羰基衍生物并入到氨中,以冷凝器作为气体收集到氨分子的数量为1以下。

著录项

  • 公开/公告号IN201718003834A

    专利类型

  • 公开/公告日2017-04-21

    原文格式PDF

  • 申请/专利权人

    申请/专利号IN201718003834

  • 发明设计人 SHINOHATA MASAAKI;MIYAKE NOBUHISA;

    申请日2017-02-02

  • 分类号C07C269;

  • 国家 IN

  • 入库时间 2022-08-21 13:38:20

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