Geranilorcinol acetylated Derivatives of compounds. Synthesis procedure for obtaining these compounds and use of these compounds as antifungals against Botrytis cinerea

摘要

Refers to a synthesis procedure for linear geranilorcinoles acetylated Derivatives of compounds, comprising: preparing a Solution mixing Orcinol (1.22 G, 9.8 mmol), geraniol (1.51 G, 98 mmol) and acetonitrile (2ml); add the previous solution in a saturated solution of acetonitrile in AgNO3 (2ml); stir the solution at room temperature under nitrogen atmosphere; Inject slowly and directly bf3et2o (0.46 G, 32 mmol); stirring for 48 hours; add Crushed Ice (approximately 30 g) and abundant salt (NaCl); Vacuum filter; extracting the Organic Phase with acoet (3 x 20 ml); washing The Organic Phase with NaHCO3 Solution (15 ml, 5%) and Water (2 x 15 ml Dry over anhydrous Na2SO4), and Evaporated to filter and Dryness. It also refers to a compound of Formula 2 and 4.This Compound is useful as Antifungal against Botrytis cinerea