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PROCESS FOR THE DIRECT SYNTHESIS OF CU-SAPO-34

机译:直接合成CU-SAPO-34的过程

摘要

Process for the direct synthesis of Cu-SAPO-34 comprising at least the following steps: preparation of a mixture containing water, at least one silicon source, at least one Al source, at least one P source, at least one Cu source, at least one 0SDA1 (where 0SDA1 is any polyamine), and at least one 0SDA2 (where OSDA2 is any organic molecule capable of directing the synthesis of the SAPO-34); and where the final synthesis mixture has the next molar composition: a Si : 0.5 Al : b P : c Cu : d OSDA1 : e OSDA2 : f H20 wherein a is in the range from 0.01 to 0.3; wherein b is in the range from 0.2 to 0.49; wherein c is in the range from 0.001 to 0.6; wherein d is in the range from 0.001 to 0.6; wherein e is in the range from 0.001 to 2; wherein f is in the range from 1 to 200; hydrothermal treatment of the mixture at 80-200°C until formation of the crystalline material, and recovery of the crystalline material.
机译:直接合成Cu-SAPO-34的方法至少包括以下步骤:制备包含水,至少一种硅源,至少一种Al源,至少一种P源,至少一种Cu源的混合物。至少一种0SDA1(其中0SDA1是任何多胺)和至少一种0SDA2(其中OSDA2是能够指导SAPO-34合成的任何有机分子);最终的合成混合物具有下一个摩尔组成:Si:0.5 Al:b P:c Cu:d OSDA1:e OSDA2:f H 2 O其中a在0.01至0.3的范围内;其中b在0.2至0.49的范围内;其中c在0.001至0.6的范围内;其中d在0.001至0.6的范围内;其中e在0.001至2的范围内;其中f在1至200的范围内;在80-200℃对混合物进行水热处理,直到形成结晶物质,并回收结晶物质。

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