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Manufacturing method of Butyldiglycol Adipate and Butyldiglycol Adipate manufactured by the same

机译:己二酸丁二二醇的制造方法和由其制造的己二酸二丁二醇酯的制造方法

摘要

The present invention relates to a method for preparing butyldiglycol adipate and butyldiglycol adipate obtained thereby. The method for preparing butyldiglycol adipate according to the present invention comprises the steps of: 1) introducing adipic acid and butyldiglycol to form a reaction mixture; 2) carrying out a primary reaction of the reaction mixture under ambiend pressure; 3) carrying out a secondary reaction of the primary reaction product under vacuum pressure; 4) cooling the secondary reaction product; and 5) neutralizing the cooled reaction product. According to the present invention, the final product is prevented from an increase in acid value, and thus the amount of waste water is reduced with a small deoxidation amount and the yield of product is increased.
机译:本发明涉及一种制备己二酸二甘醇酯的方法和由此获得的己二酸二甘醇酯。根据本发明的制备己二酸二甘醇酯的方法包括以下步骤:1)引入己二酸和二甘醇丁二醇以形成反应混合物。 2)在环境压力下进行反应混合物的初级反应; 3)在真空压力下进行一级反应产物的二级反应; 4)冷却副反应产物; 5)中和冷却的反应产物。根据本发明,防止了最终产物酸值的增加,因此以少的脱氧量减少了废水的量,并且增加了产物的产率。

著录项

  • 公开/公告号KR20170019593A

    专利类型

  • 公开/公告日2017-02-22

    原文格式PDF

  • 申请/专利权人 GEO-YOUNG CORPORATION;

    申请/专利号KR20150113592

  • 申请日2015-08-12

  • 分类号C07C51/41;C07C51/56;C07C55/14;

  • 国家 KR

  • 入库时间 2022-08-21 13:28:06

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