首页> 外国专利> / COLUMN WITH SEPARATIVE INSTALLATIONS FOR SEPARATING A MIXTURE OF HYDROCARBONS AND/OR HYDROCARBON DERIVATIVES BY MEANS OF AN EXTRACTIVE DISTILLATION USING A SELECTIVE SOLVENT

/ COLUMN WITH SEPARATIVE INSTALLATIONS FOR SEPARATING A MIXTURE OF HYDROCARBONS AND/OR HYDROCARBON DERIVATIVES BY MEANS OF AN EXTRACTIVE DISTILLATION USING A SELECTIVE SOLVENT

机译:/带有分离装置的色谱柱,通过使用选择性溶剂的萃取精馏方法分离烃和/或烃衍生物

摘要

The present invention provides an alternative solvent 2 in which the optional solvent 2 is fed to the upper column region and a mixture of the hydrocarbon and / or hydrocarbon derivative 1 to be separated is fed below the feed of the optional solvent 2, (E) for separating a mixture (1) of hydrocarbons and / or hydrocarbon derivatives by means of an extractive distillation using a distillation column (E). In column (K), the optional solvent (2) is loaded with a mixture (1) component of which the solvent has a greater affinity and the solvent is discharged from the lower column area as the loaded selective solvent (3) On the other hand, the mixture component to be separated which the selective solvent 2 has a lower affinity remains in the vapor phase and is withdrawn as the upper stream 4, which is completely or partially condensed to give a condensate 5, It is partially withdrawn as product stream 6 or returned to column K as the running return stream 7. The present invention is characterized in that a substantially horizontal first supply pipe (R1) for supplying an optional solvent is provided in the column region above the separation inner product (E) and a substantially horizontal first supply pipe (R1) Has a cross-sectional narrowing to the narrowest point (V) and is widened again after the cross-section is narrowed-open to the first feed pipe (R1) which is substantially horizontal in the region of the narrowest point (V) And a second supply pipe (R2) for supplying the return stream (7).
机译:本发明提供了替代溶剂2,其中将任选溶剂2进料至上部塔区域,并且将要分离的烃和/或烃衍生物1的混合物进料至任选溶剂2的进料下方,(E)用于通过使用蒸馏塔(E)的萃取蒸馏来分离烃和/或烃衍生物的混合物(1)。在塔(K)中,任选的溶剂(2)装载有混合物(1),该组分的溶剂具有更大的亲和力,并且该溶剂作为装载的选择溶剂(3)从下部塔区域排出。另一方面,选择性溶剂2具有较低亲和力的待分离的混合物组分保留在气相中,并作为上游料流4排出,其被完全或部分冷凝以得到冷凝物5,作为产物料流被部分排出。本发明的特征在于,在分离内部产物(E)上方的塔区域中设置有基本水平的第一供应管(R1),该第一供应管(R1)用于供给任选的溶剂,所述第一供给管(R1)设置在图6中或作为流动的回流流7返回到塔K中。基本水平的第一供应管(R1)的横截面变窄到最窄点(V),并且在横截面向基本水平的第一进料管(R1)敞开后再次变宽在最窄点(V)的区域中设有第二供应管(R2),用于供应回流(7)。

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