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Manufacturing method attached fluorine silane functional group for hexagonal and cubic mesoporous silica materials at room temperature

机译:室温下六角形和立方形介孔二氧化硅材料附着氟硅烷官能团的制备方法

摘要

The present invention relates to a process for preparing a mesoporous silica material, comprising the steps of: (a) mixing H 2 O and EtOH at a constant ratio; (b) adding a surfactant to the solution in which H 2 O and EtOH are mixed at a predetermined ratio; (c) adding a compound selected from a precursor of the mesoporous silica material and a fluorosilane functional group to the solution formed in step (b), and stirring the mixture at room temperature for a predetermined time; (d) adding ammonia water to the solution stirred in step (c) and stirring for a predetermined time; (e) washing and drying the material synthesized in the step (d) after filtration; And (f) firing after the step (e). In the present invention as described above, the carbon dioxide is chemically bonded by the fluorine group on the surface of the mesoporous silica adsorbent, so that the adsorption amount can be greatly increased.
机译:本发明涉及一种制备介孔二氧化硅材料的方法,该方法包括以下步骤:(a)以恒定的比例混合H 2 O和EtOH; (b)将H 2 O和EtOH按预定比例混合的溶液中加入表面活性剂; (c)向步骤(b)中形成的溶液中添加选自介孔二氧化硅材料的前体和氟硅烷官能团的化合物,并在室温下搅拌预定时间; (d)向步骤(c)中搅拌的溶液中加入氨水,并搅拌预定时间; (e)过滤后,洗涤并干燥步骤(d)中合成的物质; (f)在步骤(e)之后点火。在如上所述的本发明中,二氧化碳通过介孔二氧化硅吸附剂表面上的氟基团化学键合,因此吸附量可以大大增加。

著录项

  • 公开/公告号KR101723999B1

    专利类型

  • 公开/公告日2017-04-07

    原文格式PDF

  • 申请/专利权人 계명대학교 산학협력단;

    申请/专利号KR20150009537

  • 发明设计人 배재영;윤태관;구병진;

    申请日2015-01-20

  • 分类号C01B33/12;B01J20/10;

  • 国家 KR

  • 入库时间 2022-08-21 13:25:47

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