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SYNTHESIS OF ZSM-5 CRYSTALS WITH IMPROVED MORPHOLOGY
SYNTHESIS OF ZSM-5 CRYSTALS WITH IMPROVED MORPHOLOGY
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机译:形态改善的ZSM-5晶体的合成
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摘要
FIELD: physics.;SUBSTANCE: synthesis is carried out from the reaction mixtures suitable for the crystal synthesis of ZSM-12 framing structure in the absence of the seed crystals of ZSM-5 framing structure, including the absence of any seed crystals. In case of the synthesis mixtures with the sufficiently high ratio of XO2:Y2O3, the introduction of ZSM-5 seed crystals into the synthesis mixture can lead to the pure phase of ZSM-5 crystals with the new morphology. This morphology may include spiky primary crystallites of approximately 0.5 microns or less, which are ordered/aggregated into larger secondary crystalline structures.;EFFECT: primary crystallites aggregating into the secondary crystalline structure provides a large surface area of ZSM-5 crystals mesopores.;17 cl, 12 dwg, 14 tbl, 12 ex
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机译:领域:物理;实质:在不存在ZSM-5框架结构的籽晶,包括不存在任何籽晶的情况下,由适合于ZSM-12框架结构的晶体合成的反应混合物进行合成。如果合成混合物中XO 2 Sub>:Y 2 Sub> O 3 Sub>的比例足够高,则将ZSM-5晶种引入合成混合物可以产生具有新形态的ZSM-5晶体纯相。这种形态可能包括约0.5微米或更小的尖晶石初级晶体,这些晶体有序/聚集成较大的二级晶体结构。;效果:初级晶体聚集成二级晶体结构提供了大表面积的ZSM-5晶体介孔; 17 cl,12 dwg,14 tbl,12 ex
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