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METHOD FOR ANTI-ADHESIVE ANTIBACTERIAL COATING APPLICATION ON ORTHOPEDIC IMPLANTS FROM TITANIUM AND STAINLESS STEEL

机译:钛和不锈钢的骨科植入物中抗粘抗菌涂层的应用方法

摘要

FIELD: medicine.;SUBSTANCE: surface of the metal implants of titanium and stainless steel is cleaned by ion etching in a sealed chamber that is previously evacuated to a residual pressure of 9⋅10-5-1⋅10-6 Torr, followed by chamber filling with argon and chamber evacuation to a residual pressure of 4⋅10-4-1⋅10-3 Torr, and ion etching is performed with argon ions with an energy of 0.7-3.0 keV for 4-8 minutes, then an anti-adhesive antibacterial coating in the form of silver atoms and carbon in the form of tetrahedral diamond of the ta-C type is applied to the surface of orthopedic implants of titanium and stainless steel by dual spraying from two magnetron sources, using a magnetron source of carbon plasma with a power of 95-108 W, a source of silver atoms with a power of 2-20 W, and an ion source to stimulate the coating process with argon ions with inert argon gas ions energy from 0.1 to 1.5 keV, and anti-adhesive antibacterial coating application is continued in the chamber filled with argon and evacuated to a residual pressure of 4⋅10-4-1⋅10-3 Torr, while the two-component anti-adhesive antibacterial biocompatible nanocoating with a thickness of 9 to 1180 nm is applied to the metal surface of orthopedic implants containing nanogranules of spherical shape made of high-purity silver not less than 99.9% of purity, 4.5-9.5 nm in size with a continuous coating of carbon in the form of a tetrahedral diamond of ta-C type with a thickness of 0.4-1.2 nm formed on their surface. At that, graphite of the mark MPG-7, ARV or VCH is used as a magnetron source of carbon atoms for dual spraying from two magnetron sources.;EFFECT: high antiadhesive properties and high biocompatibility.;2 cl, 5 ex
机译:领域:医学;;物质:钛和不锈钢的金属植入物的表面在预先排空至9⋅10 -5 -1⋅残余压力的密闭腔室中通过离子蚀刻进行清洁10 -6 托尔,然后用氩气填充腔室并抽空至剩余压力4⋅10 -4 -1⋅10 -3 托,然后用能量为0.7-3.0 keV的氩离子进行离子刻蚀4-8分钟,然后以银原子和碳的形式以ta-的四面体金刚石的形式形成抗粘连抗菌涂层通过使用功率为95-108 W的碳等离子体磁控管,功率为2的银原子源的两个磁控管源进行双重喷涂,将C型应用于钛和不锈钢的整形外科植入物表面20 W,以及使用惰性氩气离子能量在0.1到1.5 keV之间的氩离子刺激涂层过程的离子源,并应用了抗粘连抗菌涂层在充满氩气的室内继续进行抽真空,并抽空至残余压力为4⋅10 -4 -1⋅10 -3 Torr,而两组分抗将厚度为9至1180 nm的抗菌抗菌生物相容性纳米涂层涂在整形外科植入物的金属表面上,该植入物的球形纳米颗粒由纯度不低于99.9%的高纯度银制成,尺寸为4.5-9.5 nm,并具有连续涂层在其表面形成厚度为0.4-1.2 nm的ta-C型四面体金刚石形式的碳。当时,标记为MPG-7,ARV或VCH的石墨被用作磁控管碳原子的磁源,可从两个磁控管源进行双重喷涂。效果:高抗粘性能和高生物相容性; 2 cl,5 ex

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