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Gel particle measuring method and apparatus

机译:凝胶颗粒的测定方法及装置

摘要

Provided is a gel particle measuring apparatus for detecting scattered light generated by light irradiation at a production start time point of a gel particle, and performing measurement promptly and accurately while suppressing attenuation of the scattered light in a solvent in which the phenomenon occurs. The gel particle measuring apparatus includes: a sample cell (1) configured to accommodate a sample (S) and a solution containing a reagent (R); a stirrer (2) configured to continuously stir a mixed solution (W) in the sample cell (1); a light source (3) configured to irradiate the mixed solution (W) in the sample cell (1) with coherent irradiation light (Bm); a backscattered light detector (4) configured to detect, out of light scattered in the mixed solution (W) in the sample cell (1), a backscattered light component returning toward the light source (3); a light path adjuster (5) configured to adjust an incident portion surface of the sample cell (1) so that a detection light path (ST) of, out of the light scattered in the mixed solution (W) in the sample cell (1), light traveling toward the backscattered light detector (4) is different from a reflection light path (DT) of reflection light (Bm0) reflected from a surface of the sample cell (1); and a measurement device (6) configured to determine at least a production start time point of the gel particle (G) in the mixed solution (W) based on a detection output of the backscattered light detector (4).
机译:本发明提供一种凝胶粒子测定装置,该凝胶粒子测定装置用于检测在凝胶粒子的制造开始时刻由光照射产生的散射光,并且在抑制该现象发生的溶剂中的散射光的衰减的同时,迅速且正确地进行测定。所述凝胶颗粒测量装置包括:样品室(1),其被配置为容纳样品(S)和包含试剂(R)的溶液;以及搅拌器(2),其被配置为在样品池(1)中连续搅拌混合溶液(W);光源(3),其以相干的照射光(Bm)照射样品池(1)中的混合溶液(W)。背散射光检测器(4),其被配置为从样本室(1)中的混合溶液(W)中散射的光中检测出返回光源(3)的背散射光成分;光路调节器(5),其用于调节样品池(1)的入射部分表面,使得在样品池(1)的混合溶液(W)中散射的光中的检测光路(ST) ),向后向散射光检测器(4)传播的光与从样品池(1)的表面反射的反射光(Bm0)的反射光路(DT)不同;测量装置(6),其根据背向散射光检测器(4)的检测输出,至少确定混合溶液(W)中的凝胶粒子(G)的生成开始时刻。

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