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Process for producing aryl boronic acid alkylenediol ester crystals

机译:制备芳基硼酸亚烷基二醇酯晶体的方法

摘要

PROBLEM TO BE SOLVED: To provide an economical and industrially advantageous method for obtaining an arylboronic acid alkylene diol ester of high purity, especially one having a remarkably low halogen content.SOLUTION: Provided is a method for producing a C5-25 arylboronic acid alkylene diol ester crystals, comprising: step A of producing a C5-25 aryl boronic acid alkylene diol ester by reacting a C3-20 arylboronic acid and a C2-5 alkylene diol in organic solvent; and step B of precipitating the C5-25 arylboronic acid alkylene diol ester obtained in step A in the reaction solution of the above step.
机译:解决的问题:提供一种经济和工业上有利的方法来获得高纯度的芳基硼酸亚烷基二醇酯,尤其是卤素含量极低的芳基硼酸亚烷基二醇酯。解决方案:提供了一种生产C5-25芳基硼酸亚烷基二醇的方法。酯晶体,包括:步骤A,通过使C 3-20芳基硼酸与C 2-5亚烷基二醇在有机溶剂中反应来制备C 5-25芳基硼酸亚烷基二醇酯;步骤B:在上述步骤的反应溶液中沉淀步骤A中获得的C5-25芳基硼酸亚烷基二醇酯。

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