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DESULFURIZATION PROCESS USING A COMBINATION OF A SUSPENSION BED AND A FIXED BED

机译:悬浮床和固定床结合使用的脱硫过程

摘要

Provided is a desulfurization process using a combination of a suspension bed and a fixed bed, comprising mixing the desulfurization slurry with a hydrogen sulfide containing gas to obtain a first mixture, and passing the first mixture into a suspension bed reactor from bottom to top, with controlling the first mixture to have a dwell time of 5-60 minutes in the reactor to allow they contact and react sufficiently with each other; subjecting a second mixture obtained by the reaction to gas liquid separation to produce a gas phase, feeding the gas phase into a fixed bed reactor for carrying out a second desulfurization to obtain a purified gas. The process of the present invention may reduce the sulfur content in the hydrogen sulfide containing gas from 2.4-140 g/Nm3 to 50 ppm or less by using a suspension bed, and further reduce the sulfur content to less than 10 ppm in conjunction with a fixed bed. The invention achieves high efficient desulfurization by combining the suspension bed with the fixed bed connected in series. The process of the present invention is simple and reasonable, with high desulfurization efficiency, simple equipment, little occupation of land and low investment, which is very suitable for industrial promotion.
机译:提供一种使用悬浮床和固定床的组合的脱硫方法,该方法包括将脱硫浆液与含硫化氢的气体混合以获得第一混合物,并将第一混合物从下至上进入悬浮床反应器中。控制第一混合物在反应器中的停留时间为5-60分钟,以使它们彼此接触并充分反应;使由反应获得的第二混合物进行气液分离以产生气相,将气相进料至固定床反应器中以进行第二次脱硫以获得纯化气体。本发明的方法可以通过使用悬浮床将含硫化氢的气体中的硫含量从2.4-140g / Nm 3 降低至50ppm或更低,并且进一步将硫含量降低至与固定床结合使用时小于10 ppm。本发明通过将悬浮床与固定床串联组合实现高效脱硫。本发明方法简单合理,脱硫效率高,设备简单,占地少,投资少,非常适合工业推广。

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