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METHOD FOR PREPARING SUPPORTED CATALYST FOR HETEROGENEOUS CATALYTIC OZONATION

机译:异相催化臭氧化反应中支撑催化剂的制备方法

摘要

A method for preparing a catalyst, including: 1) uniformly mixing attapulgite, lithium-manganese spinel (Li—Mn spinel), manganese dioxide powders to form mixed raw material; adding water to the mixed raw material; stirring and mixing the mixed raw material and the water for between 5 and 15 min to yield a reaction mixture; 2) feeding the reaction mixture in 1) to a pelletizer to prepare spherical particles or hollow cylindrical particles; drying the spherical particles or the hollow cylindrical particles to yield a precursor; 3) heating the precursor in a muffle furnace, and calcining the precursor to yield a crude catalyst; 4) mixing the crude catalyst with an acid solution; alternating between ultrasound and microwave to wash the crude catalyst; and 5) washing the crude catalyst in 4) with water; and drying the catalyst for 12 hrs in air at 105° C.
机译:一种催化剂的制备方法,包括:1)将凹凸棒石,锂锰尖晶石(Li-Mn尖晶石),二氧化锰粉末均匀混合,制成混合原料;向混合原料中加水;将混合的原料和水搅拌并混合5至15分钟,得到反应混合物。 2)将1)中的反应混合物加入造粒机中以制备球形颗粒或空心圆柱形颗粒;干燥球形颗粒或中空圆柱形颗粒以产生前体; 3)在马弗炉中加热前体,并煅烧前体,得到粗催化剂; 4)将粗催化剂与酸溶液混合;在超声波和微波之间交替洗涤粗催化剂。 5)将4)中的粗催化剂用水洗涤;将催化剂在105℃的空气中干燥12小时。

著录项

  • 公开/公告号US2018264457A1

    专利类型

  • 公开/公告日2018-09-20

    原文格式PDF

  • 申请/专利权人 NANJING UNIVERSITY;

    申请/专利号US201715710807

  • 发明设计人 KE XU;SHUHAN WEN;HONGQIANG REN;JINJU GENG;

    申请日2017-09-20

  • 分类号B01J37/04;B01J37/08;B01J37/06;B01J37/34;B01J21;B01J21/16;

  • 国家 US

  • 入库时间 2022-08-21 13:01:21

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