首页> 外国专利> Increasing the Sensitivity of Gas Chromatography and Gas Chromatography-Mass Spectrometry Analysis By Allowing Relatively Large Solvent Volume Injections While Reducing Sample Loss And System Contamination

Increasing the Sensitivity of Gas Chromatography and Gas Chromatography-Mass Spectrometry Analysis By Allowing Relatively Large Solvent Volume Injections While Reducing Sample Loss And System Contamination

机译:通过允许较大体积的溶剂进样,同时减少样品损失和系统污染,提高气相色谱和气相色谱-质谱分析的灵敏度

摘要

The disclosure is related to preparing a sample for chemical analysis by evaporating at least a portion of solvent included in the sample. After depositing the sample into a sample container, in some examples, at least a portion of the solvent can be evaporated. Solvent evaporation can be achieved at room temperature, at an elevated temperature, at atmospheric pressure, or by drawing a vacuum in the sample container, for example. The one or more compounds of interest can pass through a sample delivery port on the sample container into the chemical analysis device for analysis, for example. Preliminary reduction or elimination of the solvent can increase the overall amount of compounds of interest delivered into the chemical analysis device, for example. In some examples, when extra sensitivity may not be needed, less solvent can be used, which can result in a greener analytical technique that is better for the environment.
机译:本公开涉及通过蒸发样品中包括的至少一部分溶剂来制备用于化学分析的样品。在一些示例中,在将样品沉积到样品容器中之后,可以蒸发至少一部分溶剂。例如,可以在室温,升高的温度,大气压下或通过在样品容器中抽真空来实现溶剂的蒸发。例如,一种或多种目标化合物可以通过样品容器上的样品输送口进入化学分析装置进行分析。例如,溶剂的初步减少或消除会增加递送到化学分析装置中的目标化合物的总量。在某些示例中,当可能不需要额外的灵敏度时,可以使用较少的溶剂,这可以导致一种对环境更好的绿色分析技术。

著录项

  • 公开/公告号US2018246071A1

    专利类型

  • 公开/公告日2018-08-30

    原文格式PDF

  • 申请/专利权人 ENTECH INSTRUMENTS INC.;

    申请/专利号US201815908491

  • 发明设计人 DANIEL B. CARDIN;

    申请日2018-02-28

  • 分类号G01N30/12;

  • 国家 US

  • 入库时间 2022-08-21 12:57:28

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