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gentisate, adipate, trifluoroacetic acid salt, crystalline form of hydrochloride, crystalline form of besylate, amorphous besylate and processes for their preparation
gentisate, adipate, trifluoroacetic acid salt, crystalline form of hydrochloride, crystalline form of besylate, amorphous besylate and processes for their preparation
The present invention discloses a new salt of (2R)-4-oxo-4-[3-(trifluoromethyl)-5,6-dihydro[1,2,4]-triazolo[4,3-a]pyrazin-7(8H)-yl]-1-(2,4,5-trifluorophenyl)butan-2-amine (I) i.e. the gentisate salt. The invention also describes the new crystalline and amorphous forms of (2R)-4-oxo-4-[3-(trifluoromethyl)-5,6-dihydro[1,2,4]-triazolo[4,3-a]pyrazin-7(8H)-yl]-1-(2,4,5-trifluorophenyl)butan-2-amine gentisate.
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