Crystalline material with potentially optically non-linear properties, containing amino-acid and organic acid and method for obtaining the material with potentially optically non-linear properties, containing amino-acid and organic acid

摘要

crystalline potential properties optically nonlinear material containing amino acid and organic acid, is characterized by the fact that contains l - leucynu0119 and acid chloranilowy in a mole ratio of 1: 1. the material has a melting temperature of 220 - 222u00b0c and efficiency obtained was 86%.process to obtain a material containing amino acid and organic acid, is characterized by the fact that l - leucynu0119 dissolves in hot in twice distilled water, after which the aqueous solution l - leucine wkrapla chloranilowego acid solution in acetone, with the mole ratio of l - leuc yny and chloranilowego acid of 1: 1.solution the two components are mixed with a magnetic stirrer for 2 - 3 hours in the coupler 40 to 120 degrees, up to the formation of a clear homogeneous solution, filtered and leaves in access of atmospheric air at ambient temperature to slow it evaporating.after 2 - 3 weeks odsu0105cza obtained crystalline material under vacuum and subjected to a crystallization process using a mixture of double distilled water and ethanol. crystallization process is repeated several times, each time by checking the purity obtained complex by measuring the melting temperature.