Integrated set of apparatus for carrying out protonization of crystals in solutions of inorganic acids and method for conducting this reaction

摘要

an integrated set aparaturowy to carry out protonizacji crystals in solutions of inorganic acids characterised by the fact that consists of two systems, the first of which contains the tru00f3jszyjnu0105 (1) placed in the oil sump (2), standing on a heating fluid (3), with the first neck flask (1) is connected by a reflux condenser (4), a top (5), dickthe second neck flask (1) is connected (6) and the third, the thermometer (1) is connected with tube (7) through a stopcock (8) with the second, composed of the radiator inflow pipe (9), an adaptor (10) to flow through the radiator (9) and the receptacle (11).the conduct of protonizacji crystals in solutions of inorganic acids characterised by the fact that the flask (1) is inorganic acid and crystals of n, in proportion to the volume of the flask (1) introduced the acid, acid and samples heated in the bath. ejowej (2) under a reflux condenser (4), zawracaju0105c liquefied steam back into the flask (1),with temperature during heating is maintained on the level on which monitors favourably for 24 h, after which crystals removed from the flask (1) lists the przereagowany inorganic acid on his new portion, a moving again, crystals, and process powta rza.