首页> 外国专利> 7-pentoxy-naringenin and 7,4'-dipentoxy-naringenin and method for simultaneously obtaining 7-pentoxy-naringenin and 7,4'-dipentoxy-naringenin

7-pentoxy-naringenin and 7,4'-dipentoxy-naringenin and method for simultaneously obtaining 7-pentoxy-naringenin and 7,4'-dipentoxy-naringenin

机译:7-戊氧基柚皮苷和7,4'-二戊氧基柚皮苷以及同时获得7-戊氧基柚皮苷和7,4'-二戊氧基柚皮苷的方法

摘要

the object of the application is 7 - pentoksynaringenina model 2 and 7,4 '- dipontoksynaringenina model 3.the notification covers way receive these compounds, which is, to the substrate.which is naringenina model 1 the following potassium carbonate k2co3 and pentyl iodide in a mole ratio of at least 1: 1.5: 5, and the minimum amount of organic solventwhat is a reactionary, which protects against light and leaves at 20°c to 28°c for a period of 48 to 70 hours with constant stirring.then an organic solvent is vaporized, the following of a saturated solution of sodium chloride nacl and then lead extraction niemieszającym organic solvent with water.dried anhydrous magnesium sulphate and / or anhydrous sodium sulphate and the solvent vaporized, then the obtained extract is purified on column chromatography.
机译:本申请的目的是7-戊戊二醛神经递质2模型和7,4'-二烯酮体naringenina模型3,通知涵盖了将这些化合物接收到基质的方式。naringenina 1模型是以下碳酸钾k2co3和戊基碘至少1:1.5:5的摩尔比和最小量的有机溶剂是一种反应物,它可以避光并在20°C至28°C的温度下持续搅拌48至70小时。蒸发有机溶剂,然后用氯化钠氯化钠饱和溶液蒸发,然后用水萃取铅Niemieszającym有机溶剂。干燥无水硫酸镁和/或无水硫酸钠,蒸发溶剂,然后将获得的萃取液在柱上纯化层析。

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