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METHOD AND DEVICE FOR PRODUCING HIGH-MODULE LIQUID GLASS AS BINDER FOR ZINC-SILICATE COMPOSITIONS
METHOD AND DEVICE FOR PRODUCING HIGH-MODULE LIQUID GLASS AS BINDER FOR ZINC-SILICATE COMPOSITIONS
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机译:用于生产高硅酸锌组合物粘合剂的液态玻璃的方法和装置
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摘要
FIELD: chemistry.;SUBSTANCE: method for producing HMLG with a module of 3.8-4.5 and a density of 1.18-1.22 g/cm3 includes hydrothermal treatment of a suspension of finely dispersed silica with a particle size of (10-70)*10-6 m and sodium hydroxide with stirring, the process being carried out in an autoclave at the pressure of 0.0-1.5 atm and the temperature of 90-120°C, and stirring of the suspension is carried out with a stirrer (s) providing turbulent mixing of the reaction medium. The method is carried out in the device comprising an autoclave including a cylindrical vessel 1 with a lid 2, a bottom provided with a heat carrier 4 and heating elements 5, a shaft provided with a stirrer (s) 6 inside the vessel, means for loading the reagents 7, discharging the target product 8 and pouring the heat-transfer medium 9, the shaft being rotatably mounted to the stirrer (s) providing turbulent mixing of the reaction medium.;EFFECT: accelerating the brewing process.;2 cl, 1 dwg, 1 tbl
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机译:领域:化学。实质:模数为3.8-4.5且密度为1.18-1.22 g / cm 3 Sup>的HMLG的制备方法包括水热处理粒径细分散的二氧化硅悬浮液搅拌下加入(10-70)* 10 -6 Sup> m和氢氧化钠,该过程在高压釜中于0.0-1.5 atm的压力和90-120°C的温度下进行,悬浮液的搅拌用搅拌器进行,使反应介质发生湍流混合。该方法在以下装置中进行:该装置包括高压釜,该高压釜包括带有盖子2的圆柱形容器1,底部设有热载体4和加热元件5,在容器内部设有搅拌器6的轴,用于容器的装置。装入试剂7,排出目标产物8,倒入传热介质9,将轴可旋转地安装在搅拌器上,使反应介质进行湍流混合。效果:加速冲泡过程; 2 cl, 1桶,1桶
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