首页> 外国专利> INDICATOR ON MEDIA TO DETERMINE CONTENT OF SULFUR-CONTAINING COMPOUNDS IN MOTOR FUEL, METHOD FOR DETERMINING CONTENT OF SULFUR-CONTAINING COMPOUNDS IN MOTOR FUEL AND METHOD OF OBTAINING INDICATOR ON MEDIA

INDICATOR ON MEDIA TO DETERMINE CONTENT OF SULFUR-CONTAINING COMPOUNDS IN MOTOR FUEL, METHOD FOR DETERMINING CONTENT OF SULFUR-CONTAINING COMPOUNDS IN MOTOR FUEL AND METHOD OF OBTAINING INDICATOR ON MEDIA

机译:用于确定电机燃料中含硫化合物含量的介质指示剂,用于确定电机燃料中含硫化合物含量的方法以及在介质上获取指示剂的方法

摘要

FIELD: chemistry.;SUBSTANCE: indicator on the media to determine the content of sulfur-containing compounds in motor fuel includes fine sorbent with a chromogenic indicator immobilized therein. As fine sorbent, hydroxylated silica gel (98.0-99.95 wt %) is used, and as the chromogenic indicator - the indicator on the sulfur-containing compounds of chloranil (the rest). To determine the sulfur-containing compounds in motor fuel, the sample of analyzed fuel is introduced into the indicator tube filled with the indicator described above on the media by pumping or by lowering the tube into the fuel, after the end of the manifestation of the painted zone on its length the quantitative content of sulfur-containing compounds in the fuel is judged on. The method of obtaining an indicator on the media is that the chromogenic indicator is non-covalently immobilized on the sulfur-containing compounds on the fine hydroxylated silica gel by obtaining a suspension of silica gel by stirring it into a 0.05-0.2 wt % solution of chloranil at a ratio by weight of silica and solution from 1:1 to 1:10, evaporating the suspension with stirring to obtain a uniformly coloured thick mass and drying it to constant weight at a temperature of 60-80°C in case of the lack of moisture in the air.;EFFECT: invention allows to perform express analysis of the content of the sulfur-containing compounds in motor gasolines and diesel fuels.;4 cl, 1 tbl, 3 ex
机译:领域:化学。物质:用于确定汽车燃料中含硫化合物含量的介质上的指示剂,包括固定有生色指示剂的精细吸附剂。使用羟基化硅胶(98.0-99.95 wt%)作为精细吸附剂,并使用作为显色指示剂的氯苯腈含硫化合物的指示剂(其余)。为了确定汽车燃料中的含硫化合物,在燃油箱显示结束后,通过泵送或将其放低至燃油中,将分析过的燃油样品引入装有上述指示剂的指示管中。根据其长度在涂漆区域上判断燃料中含硫化合物的定量含量。在介质上获得指示剂的方法是将显色指示剂非共价固定在细羟基化硅胶上的含硫化合物上,方法是将硅胶悬浮液搅拌到0.05-0.2 wt%的硅胶和溶液的重量比为1:1的氯乙腈,搅拌下蒸发悬浮液,得到颜色均匀的浓稠物质,在60-80°C的温度下干燥至恒重空气中缺少水分。效果:本发明可以对汽车汽油和柴油中含硫化合物的含量进行明确的分析。4 cl,1 tbl,3 ex

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