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METHOD FOR PRODUCING CERAMIC POWDER BASED ON HYDROXYAPATITE AND WOLLASTONITE

机译:基于羟基磷灰石和硅灰石的陶瓷粉生产方法

摘要

FIELD: medicine.;SUBSTANCE: invention relates to medicine. Method for producing composite powders from two-component mixtures of hydroxyapatite and wollastonite, which are biocompatible with human bone tissue, while mixing aqueous solutions of calcium hydroxide, orthophosphoric acid and five-water sodium silicate, the ratio of the concentrations of the Ca/P reagents is set at 1.67, and Ca/Si = 1.00, amount of Ca(OH)2, H3PO4 and Na2SiO3 are calculated from the Ca/P and Ca/Si values and the selected proportion of hydroxyapatite/wollastonite in the powder of the desired mass, the pH is maintained at 12.00±0.05, after precipitation, the resulting solid phase is kept under the mother liquor for 24 hours at a temperature of 22–25 °C, filtered, washed with distilled water, dried at 90 °C to constant weight and calcined at 1,000 °C for 2 hours. Powders are intended for filling defects of teeth and bones in stomatology, maxillofacial surgery, traumatology, orthopedics.;EFFECT: process uses reagents that do not lead to formation of harmful by-products.;1 cl, 1 dwg, 1 tbl, 2 ex
机译:技术领域本发明涉及医学。由与人体骨组织具有生物相容性的羟基磷灰石和硅灰石的两种成分的混合物生产复合粉末的方法,同时混合氢氧化钙,正磷酸和五水硅酸钠的水溶液,Ca / P的浓度比试剂设置为1.67,并且Ca / Si = 1.00,Ca(OH) 2 ,H 3 PO 4 和Na 2 SiO 3 ,pH保持在12.00± 0.05,沉淀后,将所得固相在母液中于22-25°C下保持24小时,过滤,用蒸馏水洗涤,在90°C下干燥至恒重,并在1,000°C下煅烧2小时。粉末旨在填补口腔,颌面外科,创伤学,整形外科领域中牙齿和骨骼的缺陷;效果:该工艺使用不会导致有害副产物形成的试剂; 1 cl,1 dwg,1 tbl,2 ex

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