首页> 外国专利> METHOD FOR PRODUCING HEXAFLUOROISOPROPANOL AND FLUOROMETHYL HEXAFLUOROISOPROPYL ETHER (SEVOFLURANE)

METHOD FOR PRODUCING HEXAFLUOROISOPROPANOL AND FLUOROMETHYL HEXAFLUOROISOPROPYL ETHER (SEVOFLURANE)

机译:制备六氟异异丙醇和氟甲基六氟异丙烯醚(七氟烷)的方法

摘要

Disclosed is a method for producing a hexafluoroisopropanol, including the steps of (a) purifying a mixture containing hexafluoroacetone and at least 1,1,1-trifluoro-2,2-dichloroethane as an impurity, thereby obtaining a purified hexafluoroacetone containing 120 ppm or lower of the 1,1,1-trifluoro-2,2-dichloroethane; and (b) bringing hydrogen (H 2 ) into contact with the purified hexafluoroacetone in the presence of a catalyst, thereby hydrogenating the hexafluoroacetone into the hexafluoroisopropanol. It is possible by this method to produce the hexafluoroisopropanol with a short reaction time and a high conversion. Therefore, it is possible to particularly advantageously produce fluoromethyl hexafluoroisopropyl ether (sevoflurane) by using the hexafluoroisopropanol produced by the method.
机译:公开了一种六氟异丙醇的制造方法,该方法包括以下步骤:(a)纯化含有六氟丙酮和至少作为杂质的1,1,1-三氟-2,2-二氯乙烷的混合物,从而获得含有120ppm或以下的纯化的六氟丙酮。 1,1,1-三氟-2,2-二氯乙烷中的较低者; (b)在催化剂的存在下使氢(H 2)与纯化的六氟丙酮接触,从而将六氟丙酮氢化成六氟异丙醇。通过这种方法可以以短的反应时间和高的转化率生产六氟异丙醇。因此,通过使用由该方法生产的六氟异丙醇,可以特别有利地生产氟甲基六氟异丙基醚(七氟醚)。

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