首页> 外国专利> Polyester fiber dyeing modifier isophthalic acid synthesis method

Polyester fiber dyeing modifier isophthalic acid synthesis method

机译:聚酯纤维染色改性剂间苯二甲酸的合成方法

摘要

Polyester fiber dyeing modifier isophthalic acid synthesis method, comprises the following steps: 2 mol 2,4-diethylphenol and 4-5 mol 2,3-butanediol were added to the reaction vessel, raised the temperature of the solution to 50 to 60 V, added 2-3mol boron trifluoride piperidine 5-8 times, controlled the addition time in 130-180 min, increased the solution temperature to 65-70°C, kept for 130-150 min, and then reduced the solution temperature to 40-45 °C, added 2L trifluoroacetone solution, controlled the stirring speed at 110-130 rpm, stirred for 30-40 min, reduced the solution temperature to 5-9 V, precipitated the solid, filtered, solid was washed with p-methoxyphenol solution for 4-6 times, washed with p-methoxy benzoic acid solution for 3-5 times, combined filtrate and washing solution, adjusted the pH to 4-5with oxalic acid solution, precipitated the crystals, recrystallizated in ethylene glycol solution, dehydrated with dehydration, finally got the product isophthalic acid.
机译:聚酯纤维染色改性剂间苯二甲酸的合成方法,包括以下步骤:向反应容器中加入2摩尔的2,4-二乙基苯酚和4-5摩尔的2,3-丁二醇,将溶液的温度升至50至60V,加入2-3mol三氟化硼哌啶5-8次,控制加入时间在130-180min,将溶液温度升至65-70℃,保持130-150min,然后将溶液温度降至40-45 °C,加入2L三氟丙酮溶液,将搅拌速度控制在110-130 rpm,搅拌30-40分钟,将溶液温度降至5-9 V,沉淀出固体,过滤,将固体用对甲氧基苯酚溶液洗涤4-6次,用对甲氧基苯甲酸溶液洗涤3-5次,合并滤液和洗涤液,用草酸溶液调节pH至4-5,沉淀出晶体,在乙二醇溶液中重结晶,脱水脱水,最终得到了间苯二甲酸产品。

著录项

  • 公开/公告号IES20180092A2

    专利类型

  • 公开/公告日2019-01-09

    原文格式PDF

  • 申请/专利权人 CHENGDU ZHONG HENG HUA TIE TECHNOLOGY CO.LTD.;

    申请/专利号IES20180092

  • 发明设计人 XIANGLIANG PENG;

    申请日2018-04-03

  • 分类号C07C51/00;C07C63/00;

  • 国家 IE

  • 入库时间 2022-08-21 12:02:14

相似文献

  • 专利
  • 外文文献
  • 中文文献
获取专利

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号