Peroxide second tertbutyl Di-tert-butyl peroxide organic intermediates synthesis method

摘要

The present invention discloses peroxide second tert butyl [Di-tert-butyl peroxide] organic intermediates synthesis method, comprises the following steps:2-methyl-2-propylamine, potassium sulfate solution were added to the reaction vessel, controlled the mixing speed at 110-130rpm, controlled the reaction temperature of the solution to 5-10°C, added isopropyl alcohol aluminum, added the second glycol two ethyl ether solution in batches in 30-50min, continued to react for 90-120min;then added nickel fluoride power, controlled the mixing speed at 220-250rpm to react for 2-4h, let stand for 30-50min, layered, washed with sodium chloride solution for30-40min, washed with 1-pentanol solution for 20-40min, recrystallized in 2-hexone solution, dehydrated with dehydration, got the finished product peroxide second tert butyl.