首页> 外国专利> FIXED-BED REACTOR FOR VAPOR-LIQUID HYDROGENATION AND METHOD FOR PREPARING NEOPENTYL GLYCOL USING THE SAME

FIXED-BED REACTOR FOR VAPOR-LIQUID HYDROGENATION AND METHOD FOR PREPARING NEOPENTYL GLYCOL USING THE SAME

机译:汽液加氢的固定床反应器及使用该反应器制备新甘油的方法

摘要

The present disclosure relates to a fixed-bed gas-liquid hydrogenation reactor and a method for producing neopentyl glycol including the same, and more particularly, a plurality of holes through which a liquid raw material formed at the bottom passes and a plurality of gas raw materials passed through the bottom. A first distributor having cylindrical chimneys and cylindrical caps having a slot extending from the bottom while completely covering the chimney with a space therebetween; And a second distributor disposed below the first distribution plate at predetermined intervals and having a plurality of holes formed in the bottom thereof, wherein the height of the slot in the first distribution plate is the height of the chimney. 0.5 times or more, and the hole of the first dispersion plate is smaller than the hole of the second dispersion plate relates to a fixed bed gas-liquid hydrogenation reactor and a method for producing neopentyl glycol using the same. According to the present disclosure, through rapid mixing of the reaction raw materials and even dispersion into the catalyst layer, the catalyst utilization is increased without dead volume, so that the hydrogenation reaction yield is greatly improved, local side reactions are suppressed, and by-product formation is suppressed. In addition, there is an effect of providing a fixed-bed gas-liquid hydrogenation reactor and a process for preparing neopentyl glycol including the same, the reaction heat control being easy in a uniform reaction.
机译:固定床气液加氢反应器及其制造方法技术领域本发明涉及一种固定床气液加氢反应器及其制造方法,尤其涉及在底部形成的液体原料通过的多个孔和多个原料气。物料通过底部。第一分配器,其具有圆柱形的烟囱和圆柱形的盖,该圆柱形的盖子具有从底部延伸的狭槽,同时完全覆盖烟囱并在它们之间具有空间。第二分配器以预定的间隔设置在第一分配板的下方,并在其底部形成有多个孔,其中,第一分配板中的槽的高度为烟囱的高度。 0.5倍以上且第一分散板的孔小于第二分散板的孔涉及固定床气液加氢反应器及使用其的新戊二醇的制造方法。根据本发明,通过反应原料的快速混合以及均匀分散到催化剂层中,提高了催化剂的利用率而没有死体积,从而大大提高了氢化反应的产率,抑制了局部副反应,并且-产品形成受到抑制。此外,具有提供固定床气液氢化反应器和包括该固定床气液氢化反应器的制备新戊二醇的方法的效果,反应热的控制容易进行均匀的反应。

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