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HIGH-PERFORMANCE TEST HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY METHOD

机译:高性能测试高效液相色谱法

摘要

FIELD: medicine.;SUBSTANCE: invention relates to a method for high-performance test (HTT) high-performance liquid chromatography for testing samples of pharmaceutical compositions. Method of carrying out HPLC with high throughput comprises: lowering containers with pre-weighed samples into plastic flasks; adding the solution to each set from the container and the flasks through the dispensing nozzle of the flasks; agitation of each set of a plastic flask, a container and a solution until dissolving the sample; centrifuging each set of plastic flask, container and solution; loading an aliquot of the supernatant obtained at the centrifugation step into an HPLC column; and starting column with movable phase.;EFFECT: possibility of measuring a large volume of samples and high accuracy.;16 cl, 15 dwg, 3 tbl
机译:用于测试药物组合物样品的高性能测试(HTT)高效液相色谱方法技术领域本发明涉及一种用于测试药物组合物样品的高性能测试(HTT)高效液相色谱法。以高通量进行HPLC的方法包括:将装有预先称重的样品的容器放到塑料瓶中;通过烧瓶的分配喷嘴将溶液从容器和烧瓶加入到每组中;搅拌每组塑料瓶,容器和溶液,直至溶解样品;将每套塑料瓶,容器和溶液离心;将在离心步骤中获得的上清液的等分试样装入HPLC柱中;效果:可以测量大量样品并且具有很高的准确性; 16 cl,15 dwg,3 tbl

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