首页> 外国专利> PROCESS FOR THE PREPARATION OF A MESOPOROUS ALUMINA FROM A CONTINUOUSLY PREPARED DISPERSIBLE GEL AND WITHOUT GROWING DRYING

PROCESS FOR THE PREPARATION OF A MESOPOROUS ALUMINA FROM A CONTINUOUSLY PREPARED DISPERSIBLE GEL AND WITHOUT GROWING DRYING

机译:从连续制备的分散凝胶中制备无孔氧化铝的方法

摘要

A process for preparing a mesoporous alumina comprising a) at least a first step of precipitating alumina, at least one basic precursor and at least one acid precursor in which at least one of the basic precursors is described. or acid comprises aluminum, at a pH of the reaction medium of between 6 and 10, at a temperature of between 40 and 95 ° C., said step a) being carried out without backmixing, b) a step of heat treatment of the suspension obtained at the end of step a) at a temperature of between 50 and 200 ° C., c) a filtration step of the suspension obtained followed by at least one washing step of the gel obtained, d) a step of removing at least a portion of the water of said alumina gel obtained at the end of step c) at a temperature below 50 ° C e) a step of shaping-extrusion formed with an acid level of between 0 and 4% and a neutralization rate of is between 0 and 100%, f) a heat treatment step at a temperature between 500 and 1000 ° C, in the presence or absence of a flow of air containing up to 60% by volume of water.
机译:一种制备中孔氧化铝的方法,其包括a)至少使氧化铝沉淀的第一步,至少一种碱性前体和至少一种酸前体,其中描述了至少一种碱性前体。或酸包含铝,在6至10的反应介质的pH下,在40至95℃的温度下,所述步骤a)不进行回混即可进行,b)悬浮液的热处理步骤在步骤a)结束时在50至200°C的温度下获得的溶液; c)所获得的悬浮液的过滤步骤,随后是所获得凝胶的至少一个洗涤步骤,d)除去至少一个在步骤c)结束时在低于50°C的温度下获得的所述氧化铝凝胶的一部分水e)酸含量为0%至4%且中和率为0%的成型挤压步骤100%,f)在存在或不存在包含高达60体积%的水的空气流的情况下在500至1000℃之间的温度下的热处理步骤。

著录项

  • 公开/公告号FR3067021A1

    专利类型

  • 公开/公告日2018-12-07

    原文格式PDF

  • 申请/专利权人 IFP ENERGIES NOUVELLES;

    申请/专利号FR20170054906

  • 申请日2017-06-02

  • 分类号C01F7/34;B01J20/08;B01J21/04;B01J32;B01J37/03;

  • 国家 FR

  • 入库时间 2022-08-21 11:43:56

相似文献

  • 专利
  • 外文文献
  • 中文文献
获取专利

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号