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SYNTHESIS OF NANOCRYSTALLINE MFI ZEOLITE, SYNTHESIS METHOD AND USE THEREOF IN CATALYTIC APPLICATIONS

机译:纳米MFI沸石的合成,合成方法及其在催化应用中的用途

摘要

The present invention relates to a new process for synthesising a crystalline material comprising the zeolite MFI structure in nanocrystalline form, and which can comprise at least the following steps: i) preparing a mixture comprising at least one source of water, at least one source of a tetravalent element Y, at least one source of a trivalent element X, at least one source of an alkali cation or alkaline earth metal cation (A), and at least one organic molecule (OSDA1), wherein OSDA1 is preferably a monocyclic quaternary ammonium with the structure R1R2CycloN+, the molar composition of the mixture being: n X2O3 : YO2: a A : m OSDA1 : z H2O; ii) crystallising this mixture in a reactor; and iii) recovering the crystalline material obtained.
机译:本发明涉及合成包含纳米晶形式的沸石MFI结构的晶体材料的新方法,该方法可以包括至少以下步骤:i)制备包含至少一种水源,至少一种水源的混合物。四价元素Y,三价元素X的至少一种来源,碱金属阳离子或碱土金属阳离子的至少一种来源(A)和至少一种有机分子(OSDA1),其中OSDA1优选为单环季铵盐结构为R 1 R 2 CycloN + ,混合物的摩尔组成为: n X 2 O 3 :YO 2 :a A: m OSDA1: z H 2 O; ii)在反应器中使该混合物结晶; iii)回收获得的结晶材料。

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