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Titanium Sub-oxide/Ruthenium Oxide Composite Electrode And Preparation Method And Application Thereof

机译:氧化钛/氧化钌复合电极及其制备方法和应用

摘要

A titanium sub-oxide/ruthenium oxide composite electrode and a preparation method and application thereof. Titanium-based titanium sub-oxide nanotubes is taken as a bottom layer, and titanium sub-oxide doped ruthenium oxide is taken as a surface composite active layer. A titanium substrate is anodized in a fluorine-containing ionic electrolyte, taken out, subjected to heating and roasting, cooled and then subjected to cathodic electrochemical reduction in polarizing liquid, so that a titanium-based titanium sub-oxide nanotube electrode is obtained; and then the titanium-based titanium sub-oxide nanotube electrode is taken as a cathode to be electrodeposited in a ruthenium trichloride electrolyte doped with titanium sub-oxide powder, taken out and then subjected to heating and roasting, so that the titanium sub-oxide/ruthenium oxide composite electrode is obtained.
机译:氧化钛/氧化钌复合电极及其制备方法和应用。将钛基钛亚氧化物纳米管作为底层,并将掺杂钛亚氧化物的氧化钌作为表面复合活性层。钛基板在含氟离子电解质中进行阳极氧化,取出后进行加热焙烧,冷却,然后在偏光液中进行阴极电化学还原,得到钛基钛亚氧化物纳米管电极。然后以钛基钛亚氧化物纳米管电极为阴极,电沉积在掺有钛亚氧化物粉末的三氯化钌电解液中,取出并进行加热焙烧,得到钛亚氧化物。得到氧化钌复合电极。

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