首页> 外国专利> PLUG FLOW DISTILLATION TRAY AND METHOD FOR PREPARING ISOPHORON BY LIQUID-PHASE CONDENSATION OF ACETONE

PLUG FLOW DISTILLATION TRAY AND METHOD FOR PREPARING ISOPHORON BY LIQUID-PHASE CONDENSATION OF ACETONE

机译:丙酮液相凝结的料流蒸馏塔板及制备异丙苯的方法

摘要

The present invention provides a plug flow distillation tray and a method for preparing isophorone by liquid-phase condensation of acetone. The plug flow distillation tray provided by the present invention comprises a tray and a plug flow assembly provided on the tray, the plug flow assembly comprising a downcomer, a leveled overflow weir, a light-heavy phase flow dividing element, a liquid receiving tray I and a flow guide element; the downcomer is connected to the tray, and the leveled overflow weir is provided on an inlet of the downcomer; the light-heavy phase flow dividing element is provided in the downcomer and is located below the leveled overflow weir; the liquid receiving tray I is connected to the tray, and is located on a side opposite to the side where the downcomer is connected to the tray; the flow guide element is provided above the junction of the liquid receiving tray I and the tray, and the flow guide element is provided with a plurality of flow guide passages. A pressurized reactive distillation column comprising the plug flow distillation tray of the present invention can be used for performing post-treatment of an IP (isophorone)/alkali liquid system which is easy to foam, so that the liquid phase can be distributed and flow relatively evenly, thereby facilitating the improvement of the reaction effect.
机译:本发明提供了一种活塞流蒸馏塔板和一种通过丙酮液相缩合制备异佛尔酮的方法。本发明提供的活塞流蒸馏塔板,包括塔板和设置在该塔板上的活塞流组件,所述活塞流组件包括降液管,水平溢流堰,轻重相流分配元件,液体接收塔板I。以及导流元件;降液管与塔盘相连,在降液管的进口设有水平溢流堰。轻重相分流元件设置在降液管中,并位于水平溢流堰的下方。液体接收托盘I连接到托盘,并且位于与降液管连接到托盘的一侧相反的一侧;导流元件设置在液体接收托盘I和托盘的接合部的上方,并且导流元件设置有多个导流通道。包括本发明的活塞流蒸馏塔板的加压反应蒸馏塔可以用于对易于起泡的IP(异佛尔酮)/碱液体体系进行后处理,使得液相可以相对地分布和流动。均匀地促进反应效果的提高。

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