首页> 外国专利> METHOD FOR SYNTHESIZING METAL ION-DOPED CERIA USING SOLVOTHERMAL SYNTHESIS

METHOD FOR SYNTHESIZING METAL ION-DOPED CERIA USING SOLVOTHERMAL SYNTHESIS

机译:溶剂热合成法合成金属掺杂铈的方法

摘要

The present invention relates to a method for preparing metal ion-doped seria, including the steps of: (a) adding a basic material to cerium acetate solution to modify pH; (b) adding a basic material to a metal ion precursor solution to modify pH; and (c) dispersing each of the solutions obtained from steps (a) and (b) in a solvent, and carrying out solvothermal reaction at a temperature of 90-160°C to form metal ion-doped seria. According to the present invention, it is possible to prepare metal ion-doped seria having a high specific surface area and crystallinity at a temperature (90-160°C) lower than the conventional hydrothermal synthesis temperature in a cost-efficient manner through a solvothermal synthesis process without any surfactant or additional heat treatment. Particularly, the specific surface area of metal ion-doped serial can be improved significantly by using cerium acetate as a cerium precursor.
机译:本发明涉及一种制备金属离子掺杂的二氧化铈的方法,该方法包括以下步骤:(a)在醋酸铈溶液中加入碱性物质以调节pH值; (b)在金属离子前体溶液中加入碱性物质以改变pH值; (c)将由步骤(a)和(b)获得的每种溶液分散在溶剂中,并在90-160℃的温度下进行溶剂热反应以形成掺杂金属离子的二氧化铈。根据本发明,可以通过溶剂热以节省成本的方式制备在比常规水热合成温度低的温度(90-160℃)下具有高比表面积和结晶度的掺杂金属离子的二氧化铈。合成过程中无需任何表面活性剂或额外的热处理。特别地,通过使用乙酸铈作为铈前体,可以显着提高掺杂金属离子的系列的比表面积。

著录项

相似文献

  • 专利
  • 外文文献
  • 中文文献
获取专利

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号