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APPARATUS AND METHOD FOR PRODUCING DISPERSIONS AND SOLIDS

机译:产生色散和固体的设备和方法

摘要

The present invention relates to an apparatus and method for producing dispersions and solids by controlled precipitation, coprecipitation and self-organization processes in a microjet reactor, wherein the jet of a solvent (2) comprising at least one target molecule is At the impact point (K) of the reactor chamber of the reactor collides with the jet of non-solvent (3) at a prescribed pressure and flow rate, and the microjet reactor has a gas inlet (5) and gas for introducing gas into the reactor chamber (1) It has a reactant outlet 6 for discharging the reactants into a stream of. This leads to very rapid precipitation, coprecipitation or chemical reactions in which microparticles or nanoparticles are produced. In order to provide an apparatus capable of performing solvent/non-solvent precipitation to produce as small particles as possible and not significantly affected by Ostwald ripening in the resulting dispersion, the present invention provides a spray-drying unit 7 at the outlet of the reactant. It is proposed to provide a control circuit 11 to connect and optimize and maintain the operating parameters of the spray-drying unit 7.
机译:本发明涉及在微喷射反应器中通过受控的沉淀,共沉淀和自组织过程生产分散体和固体的设备和方法,其中包含至少一个目标分子的溶剂(2)的喷射在冲击点(反应器反应室的K)在规定的压力和流速下与非溶剂(3)的射流相撞,并且微喷射反应器具有进气口(5)和用于将气体引入反应室(1)的气体)具有用于将反应物排放到其中的反应物出口6。这导致非常快速的沉淀,共沉淀或化学反应,其中产生微粒或纳米颗粒。为了提供一种能够进行溶剂/非溶剂沉淀以产生尽可能小的颗粒并且在所得分散体中不受奥斯特瓦尔德熟化的显着影响的设备,本发明在反应物的出口提供了喷雾干燥单元7。 。建议提供控制电路11以连接并优化和维持喷雾干燥单元7的操作参数。

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