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Microstructure evolution of AA7050 Al alloy during Equal-Channel Angular Pressing

机译:等径角挤压过程中AA7050铝合金的组织演变

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摘要

High strength AA7050 aluminum alloy was processed by ECAP through route A in the T7451 condition. Samples were processed at 423 K, with 1 and 3 passes. The resulting microstructure was evaluated by optical microscopy (OM), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The phases were identified by X-ray diffraction (XRD) using monochromatic Cu Kα radiation. Rockwell B hardness and tensile tests were performed for assessment of mechanical properties. The microstructure was refined by the formation of deformation bands, with dislocation cells and elongated subgrains, with an average width of 240 nm, inside these bands. The number of deformation bands increased with the number of passes. A reduction of precipitates size was observed with increase in the number of passes, when compared to initial condition, probably resulting from particle fragmentation during ECAP. After three passes the precipitates tend to a more equiaxed morphology and have sizes smaller than 10 nm. Phases Η' and Η coexist in the microstructure, but Η is the dominant phase, mainly after three passes. The hardness of alloy after the first pass of ECAP is almost equal to the initial condition. After three passes the hardness showed a slight reduction which must be result from recovery process. There was a slight improvement in the yield strength and elongation after one pass, when compared to the initial T7451 condition. The improvement in the ultimate tensile strength was less significant.
机译:ECAP在T7451条件下通过路线A对高强度AA7050铝合金进行了加工。样品在423 K下经过1和3遍处理。通过光学显微镜(OM),扫描电子显微镜(SEM)和透射电子显微镜(TEM)评估所得的微观结构。通过使用单色CuKα辐射的X射线衍射(XRD)识别相。进行了洛氏硬度和硬度测试以评估机械性能。通过形变带的形成来细化微观结构,形变带内有位错单元和细长的亚晶粒,平均宽度为240 nm。变形带的数量随着通过的次数而增加。与初始条件相比,随着通过次数的增加,观察到沉淀物尺寸的减小,这可能是由于ECAP期间的颗粒破碎所致。经过三遍后,沉淀物趋于等轴形态,尺寸小于10 nm。在显微组织中共存有H'相和H相,而H是主要相,主要在三遍通过后。 ECAP第一次通过后的合金硬度几乎等于初始条件。经过三遍后,硬度略有降低,这必须归因于恢复过程。与最初的T7451条件相比,经过一遍后屈服强度和伸长率略有改善。极限抗拉强度的改善不太明显。

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