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NEW CERAMICS SURFACE REINFORCING TREATMENT USING A COMBINATION OF CRACK-HEALING AND ELECTRON BEAM IRRADIATION

机译:裂纹愈合与电子束辐照相结合的新型陶瓷表面处理

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摘要

New surface reinforcement using a combination of crack-healing and electron beam irradiation is proposed for structural ceramics. The influence of electron beam irradiation on the surface hardness was investigated in the present study. Hot-pressed alumina-30 vol. % SiC particles composite was crack-healed, via a high-temperature oxidation treatment in air at 1573 K for 1 h. Then, the specimens passed through an electron beam curtain to homogeneously irradiate the crack-healed specimens. The total dose of irradiation was controlled by repeating the procedure. Depth profiles of hardness were measured using Vickers indentation with several indented loads. The hardness of the electron beam irradiated specimens increased from that of crack-healed specimens without electron beam irradiation in the vicinity of the surface. The depth influenced by electron beam irradiation was found to be about 2 urn. Irradiation of 0.432 MGy caused a 38 % hardness increment to surface of the crack-healed specimens. A similar irradiation effect was achieved in non crack-healed specimen. The hardness in the vicinity of the surface varied with electron beam irradiation dose and the optimized conditions of electron beam irradiation to crack-healed and non crack-healed specimens were determined to be 0.432 MGy and 0.216 MGy, respectively.
机译:提出了结合裂纹愈合和电子束辐照的新型表面增强材料,用于结构陶瓷。在本研究中研究了电子束辐照对表面硬度的影响。热压氧化铝30卷通过在1573 K的空气中进行高温氧化处理1小时,对%SiC颗粒复合材料进行了裂纹修复。然后,样品通过电子束帘幕均匀地照射裂纹愈合的样品。通过重复该过程来控制照射的总剂量。硬度的深度分布是使用带有多个压痕载荷的维氏压痕测量的。与在表面附近不进行电子束照射的情况下,经电子束照射的样品的硬度相比,在未进行电子束照射的情况下,裂纹恢复的样品的硬度增加。发现受电子束照射影响的深度为约2μm。照射0.432 MGy可使裂纹愈合的试样表面硬度增加38%。在未裂纹愈合的样品中也获得了类似的辐照效果。表面附近的硬度随电子束辐照剂量而变化,并且对裂纹愈合和未裂纹愈合的样品的电子束辐照的最佳条件分别确定为0.432 MGy和0.216 MGy。

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