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Alumina-copper joining by the sintered metal powder process

机译:通过烧结金属粉末工艺进行氧化铝-铜连接

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摘要

Sintered metal powder process (SMPP) is one of the high technology methods in ceramic-metal joining domain. The present study examines the effect of temperature and time of metalized layer sintering on the thickness and homogeneity of the joining layer, the leakage rate in alumina-copper joining zone, and also identifies the different phases formed during sintering. The samples were characterized by optical microscopy (OM), scanning electron microscopy (SEM) and energy dispersion spectroscopy (EDS). Microstructure studies indicate that sintering the metalized layer with a holding time of 90 min at the temperature of 1530 deg C, and with an applied layer thickness of 50 |xm with proper plating and brazing stages lead to a completely homogeneous joining zone with an adequate thickness (about 33 mu m). The results of leak tests on alumina-copper specimen in this condition was less than 10~(-9)Pa 1 s~(-1).
机译:烧结金属粉末工艺(SMPP)是陶瓷-金属连接领域中的一种高科技方法。本研究研究了金属化层烧结的温度和时间对连接层的厚度和均匀性,氧化铝-铜连接区的泄漏率的影响,并确定了烧结过程中形成的不同相。通过光学显微镜(OM),扫描电子显微镜(SEM)和能量分散光谱(EDS)对样品进行表征。微观结构研究表明,在1530摄氏度的温度下,以90分钟的保持时间烧结金属化层,并通过适当的电镀和钎焊步骤,以50 | xm的施加层厚度对金属化层进行烧结,可以得到具有足够厚度的完全均匀的接合区域(约33微米)。在此条件下对氧化铝-铜试样的泄漏测试结果小于10〜(-9)Pa 1 s〜(-1)。

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