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Preparation of TiO2 nano-particle photocatalysts by a multi-gelation method: the effect of pH change

机译:多凝胶法制备TiO2纳米粒子光催化剂:pH变化的影响

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摘要

TiO2 photocatalysts were prepared by a multi-gelation method and the effect of the changes in the PH during the PH swing times, i.e., by a controlled PH swing, on the morphology of the TiO2 particles was investigated. The photocatalytic properties of the Ti02 catalysts prepared by controlled PH swing were compared with TiO2 Particles prepared without adjusting the PH during the swing times. The photocatalytic degradation reaction of these TiO2 catalysts was investigated by comparing their effectiveness in 2-propanol oxidation. The experimental results showed that the TiO2 photocatalysts prepared without adjusting the PH performed better in controlling the important parameters of the catalysts such as particle size, surface area, anatase/rutile phase ratio and pore size, as well as pore volume than the TiO2 photocatalysts prepared by a controlled pH swing method.
机译:通过多凝胶化方法制备了TiO 2光催化剂,并且研究了在PH摆动时间内,即通过控制的PH摆动,PH的变化对TiO 2颗粒形态的影响。将通过控制PH摆动制备的TiO2催化剂的光催化性能与在摆动时间内未调节PH的TiO2颗粒进行了比较。通过比较它们在2-丙醇氧化中的有效性,研究了这些TiO2催化剂的光催化降解反应。实验结果表明,与制备的TiO2光催化剂相比,无需调节PH值制备的TiO2光催化剂在控制催化剂的重要参数(例如粒径,表面积,锐钛矿/金红石相比和孔径以及孔体积)方面表现更好。通过控制pH摆动法。

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