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Detection of hydrogen leakage in a composite sandwich structure at cryogenic temperature

机译:低温下复合材料夹层结构中的氢泄漏检测

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摘要

Hydrogen tanks made of polymer-matrix composite material have been proposed as an enabling technology for reducing the weight of reusable launch vehicles and increasing their payload. A key development issue for these lightweight structures is the leakage of hydrogen through the composite material, which is generally a function of the tank material, manufacturing method, mechanical load, any internal damage states in the material, and the temperatures at which the tank must operate. A method for measuring leakage through a geometrically complex structure at cryogenic temperatures and under mechanical load that has been developed, calibrated, and used to measure helium and hydrogen leakage through the X-33 liquid hydrogen tank structure is presented. In particular, results from the calibration tests are presented that indicate that the measurement errors are less than 10 for leak rates ranging from 0.3 to 200 cm(3)/min at standard atmospheric conditions. In addition, both hydrogen and helium leak tests that were performed on two specimens taken from a discarded segment of the X-33 tank structure and results are compared. For both the hydrogen and helium tests leak rates varied with the applied mechanical load. The level of hydrogen leakage is shown to be significantly higher than the helium leakage and to exceed the acceptable leak rate for a vehicle like the X-33 liquid hydrogen tank by an order of magnitude. References: 8
机译:由聚合物基复合材料制成的氢气罐已被提议作为减轻可重复使用运载火箭重量和增加其有效载荷的使能技术。这些轻质结构的一个关键开发问题是氢气通过复合材料的泄漏,这通常是储罐材料、制造方法、机械载荷、材料中的任何内部损坏状态以及储罐必须运行的温度的函数。提出了一种在低温和机械载荷下测量几何复杂结构泄漏的方法,该方法已被开发、校准并用于测量通过 X-33 液氢罐结构的氦气和氢气泄漏。特别是,校准测试的结果表明,在标准大气条件下,泄漏率范围为0.3至200 cm(3)/min,测量误差小于10%。此外,还比较了对从X-33储罐结构的废弃部分采集的两个样品进行的氢气和氦气泄漏测试以及结果。对于氢气和氦气测试,泄漏率随施加的机械载荷而变化。氢气泄漏水平明显高于氦气泄漏水平,并且比X-33液氢罐等车辆的可接受泄漏率高出一个数量级。[参考资料: 8]

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