Synthesis of sarcodictyin A analogue containing 14-methyl group and C(12)=C(13) bond in ring A from levoglucosenone

Sharipov Bulat T.; Pershin Alexey A.; Valeev Farid A.

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Synthesis of sarcodictyin A analogue containing 14-methyl group and C(12)=C(13) bond in ring A from levoglucosenone

机译：左旋葡糖苷环A中含有14-甲基和C（12）=C（13）键的肌苇素A类似物的合成

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摘要

Starting from levoglucosenone piperilene Diels-Alder adduct a total synthesis of sarcodictyin A analogue containing 14-methyl group and C(12)=C(13) bond in ring A was performed, where the key step was the intramolecular cyclization between acetylene and aldehyde moieties to produce a 10-membered carbocycle.

机译：从左旋葡萄糖苑哌啶开始，Diels-Alder加合物在环A中合成了含有14-甲基和C（12）=C（13）键的肌炔素A类似物，其中关键步骤是乙炔和醛部分之间的分子内环化反应，以产生10元碳环。

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来源
《Mendeleev Communications 》 |2017年第2期| 119-121| 共3页
作者
Sharipov Bulat T.; Pershin Alexey A.; Valeev Farid A.;
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Russian Acad Sci, Ufa Inst Chem, Ufa 450054, Russia;

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正文语种英语
中图分类化学 ;
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Synthesis of sarcodictyin A analogue containing 14-methyl group and C(12)=C(13) bond in ring A from levoglucosenone

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