首页> 外文期刊>journal of applied physics >Transmission sputtering of gold thin films by low‐energy (<1 keV) xenon ions. I. The system and the measurement
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Transmission sputtering of gold thin films by low‐energy (<1 keV) xenon ions. I. The system and the measurement

机译:通过低能(<1 keV)氙离子对金薄膜进行透射溅射。一、系统与测量

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摘要

A novel system for direct measurement of the transmission‐sputtering yields of ion‐irradiated thin films is described. The system was specifically designed for the study of the transmission sputtering caused by low‐energy (<1 keV) xenon ions. The xenon ion beam employed is first mass‐analyzed in a specially constructed corssed magnetic‐ and electric‐field mass spectrometer; this analyzer eliminates all energetic neutral and singly charged ions of mass less than 40 amu; it is also expected that ≤2 of the xenon ions which actually reach a specimen are doubly charged. The analyzed xenon ion beam is made to impinge on a gold thin film (∼100–500 A˚ thick) which is mounted in a JEM 200 transmission electron‐microscope holder. The temperature of the specimen can be varied between ∼25 and 300 K employing a continuous transfer liquid‐helium cryostat. The particles (atoms or ions) ejected from theunirradiatedsurface of the gold thin film are detected by two channeltron electron‐multiplier arrays (CEMA) in the Chevron configuration; the Chevron detector is able to detect individual transmission‐sputtered particles when operated in the saturated mode. To further enhance resolution, the electron cascades (produced by the CEMA), are amplified and shaped electronically into uniform square pulses. The shaped signals are detected with an Ithaco 391A lock‐in amplifier (LIA). With the aid of a ratiometer feature in the LIA, we are able to measure directly the ratio of the transmission‐sputtered currentItto the incident ion currentIb; forIbn=1 mgr;A cm−2, a ratio ofIt/Ibas small as 1×10−9has been measured. A detailed discussion of the calibration procedure and the experimental errors, involved in this technique, are also presented.
机译:描述了一种用于直接测量离子辐照薄膜的透射率和连字符溅射产率的新系统。该系统专门设计用于研究由低能量(<1 keV)氙离子引起的透射溅射。所采用的氙离子束首先在特制的磁性质谱仪和电场质谱仪中进行质谱分析;该分析仪可消除所有质量小于 40 amu 的高能中性和单电荷离子;还预计实际到达样品的氙离子中≤2&Percnt;带双重电荷。分析的氙离子束被制成撞击金薄膜(∼100–500 A&环厚),该薄膜安装在JEM 200透射电子显微镜支架中。试样的温度可以在 ∼25 到 300 K 之间变化,采用连续转移液体&连字符;氦气低温恒温器。从金薄膜的未辐照表面喷射出的粒子(原子或离子)由雪佛龙配置中的两个通道电子和连字符倍增器阵列(CEMA)检测;雪佛龙探测器在饱和模式下工作时能够检测单个透射溅射颗粒。为了进一步提高分辨率,电子级联(由CEMA产生)被放大并以电子方式塑造成均匀的方脉冲。整形信号通过Ithaco 391A锁连字符放大器(LIA)进行检测。借助LIA中的比率计功能,我们能够直接测量透射溅射电流与入射离子电流Ib的比率;对于 Ibn=1 &mgr;A cm−2,已测量出小至 1×10−9 的 It/Ibas 之比。还详细介绍了该技术中涉及的校准程序和实验误差。

著录项

  • 来源
    《journal of applied physics》 |1982年第10期|6968-6978|共页
  • 作者

    Guy Ayrault; David N. Seidman;

  • 作者单位
  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 英语
  • 中图分类
  • 关键词

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