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Densification behavior, microstructure evolution, and wear performance of selective laser melting processed commercially pure titanium

机译:商业纯钛选择性激光熔化加工的致密化行为、微观结构演变和磨损性能

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摘要

This work presents a comprehensive study of the densification behavior, phase and microstructure development, hardness and wear performance of commercially pure Ti parts processed by selective laser melting (SLM). An in-depth relationship between SLM process, microstractures, properties, and metallurgical mechanisms has been established. A combination of a low scan speed and attendant high laser energy density resulted in the formation of microscopic balling phenomenon and interlayer thermal microcracks, caused by a low liquid viscosity, a long liquid lifetime, and resultant elevated thermal stress. In contrast, using a high scan speed produced the disorderly liquid solidification front and considerably large balling, due to an elevated instability of the liquid induced by Marangoni convection. A narrow, feasible process window was accordingly determined to eliminate process defects and result in full densification. The phase constitutions and microstructural characteristics of SLM-processed Ti parts experienced a successive change on increasing the applied scan speeds: relatively coarsened lath-shaped a -> refined acicular-shaped martensitic a' -> further refined zigzag-structured martensitic a', due to the elevated thermal and kinetic undercooling and attendant solidification rate. The optimally prepared fully dense Ti parts had a very high hardness of 3.89 GPa, a reduced coefficient of friction of 0.98 and wear rate of 8.43 x 10"4 mm3 N"1 m^1 in dry sliding wear tests. The formation of an adherent, plastically smeared tribolayer on the worn surface contributed to the enhancement of wear performance.
机译:这项工作对通过选择性激光熔化 (SLM) 加工的商业纯钛零件的致密化行为、相和微观结构发展、硬度和磨损性能进行了全面研究。SLM工艺、微观牵引、性能和冶金机理之间建立了深入的关系。低扫描速度和随之而来的高激光能量密度相结合,导致形成微观球状现象和层间热微裂纹,这是由于液体粘度低、液体寿命长以及由此产生的热应力升高所致。相比之下,由于马兰戈尼对流引起的液体不稳定性增加,使用高扫描速度会产生无序的液体凝固前沿和相当大的球状。因此,我们确定了一个狭窄、可行的工艺窗口,以消除工艺缺陷并实现完全致密化。随着扫描速度的提高,SLM加工钛零件的相构成和微观结构特征发生了连续变化:由于热和动能过冷的升高以及随之而来的凝固速率升高,相对粗化的板条形a->精制针状马氏体a'->进一步精细的锯齿形结构马氏体a'。在干滑磨损试验中,经过优化制备的全致密钛零件具有 3.89 GPa 的非常高的硬度、0.98 的摩擦系数和 8.43 x 10“4 mm3 N”1 m^1 的磨损率。在磨损表面上形成粘附的、涂有塑性的摩擦层有助于提高磨损性能。

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