In this paper we report the synthesis and study of the first examples of oxomolybdenum (V) complexes with di-#x3BC;-sulphido bridges and n-pentyl, n-hexyl, n-heptyl, iso-octyl, cyclohexyl and phenyl carboxylates as ligands. The complexes have been characterized by analytical, magnetochemical, IR and visible-UV spectral methods and are assigned the formula Mo2O2S2(RC02)2.
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